HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Bromo-4-methoxy-1H-indole → 4-(6-bromo-4-methoxy-1H-indol-1-yl)-6-chloro-2,3-dimethylquinoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Bromo-4-methoxy-1H-indole | HCID 24728034 | — |
| Reactant | 4,6-Dichloro-2,3-dimethylquinoline | HCID 60994963 | — |
| Product | 4-(6-bromo-4-methoxy-1H-indol-1-yl)-6-chloro-2,3-dimethylquinoline | HCID 67285059 | — |
Reaction Steps
Prepared according to procedure U using 6-bromo-4-methoxy-1H-indole (0.05 g, 0.22 mmol) and 4,6-dichloro-2,3-dimethylquinoline (0.075 g, 0.33 mmol) to give 4-(6-bromo-4-methoxy-1H-indol-1-yl)-6-chloro-2,3-dimethylquinoline as a yellow solid: Mass Spectrum (ESI) m/e=415.0 [M+1 (79Br)] and 417.0 [M+1 (81Br)].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765940B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-522b3c3d025c4aa98d56232c3b0cae1b |
| Source note | uspto-grants-2014_07 |