HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Bromo-1H-indole-4-carbonitrile → 6-bromo-1-(6-chloro-2,3-dimethylquinolin-4-yl)-1H-indole-4-carbonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Bromo-1H-indole-4-carbonitrile | HCID 24728609 | — |
| Reactant | 4,6-Dichloro-2,3-dimethylquinoline | HCID 60994963 | — |
| Product | 6-bromo-1-(6-chloro-2,3-dimethylquinolin-4-yl)-1H-indole-4-carbonitrile | HCID 67285353 | — |
Reaction Steps
Prepared according to procedure U using 6-bromo-1H-indole-4-carbonitrile (0.5 g, 2.26 mmol) and 4,6-dichloro-2,3-dimethylquinoline (0.5626 g, 2.49 mmol) to give 6-bromo-1-(6-chloro-2,3-dimethylquinolin-4-yl)-1H-indole-4-carbonitrile as a yellow solid: Mass Spectrum (ESI) m/e=410.0 [M+1 (79Br)] and 412.0 [M+1 (81Br)].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765940B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-ec23b8c9a5584de89c00f3ab5b33afcf |
| Source note | uspto-grants-2014_07 |