Triacetoxyperiodinane → HCID 70968164, compound

Participants

Reaction Steps

0.15 g of 1-[2-fluoro-6-(8-fluoroquinolin-3-yloxy)-phenyl]-2-methyl-propane-1,2-diol was dissolved in 10 ml of dichloromethane, and 0.20 g of Dess-Martin reagent was added thereto at 0° C. After 2 hours of stirring, the reaction solution was concentrated and purified by silica gel column chromatography to obtain 0.03 g of 1-[2-fluoro-6-(8-fluoroquinolin-3-yloxy)-phenyl]-2-hydroxy-2-methyl-propan-1-one (Compound Number 398).

Provenance & Evidence