Ethanolamine → HCID 178518158, compound

HRID 1620721Notes

Reaction equation

HRID 1620721 reaction equation
S=[C:2]1[CH2:6][S:5][C:4](=[O:7])[NH:3]1.[NH2:8][CH2:9][CH2:10][OH:11]>C(O)C>[OH:11][CH2:10][CH2:9][NH:8][C:2]1[CH2:6][S:5][C:4](=[O:7])[N:3]=1

Participants

4

Reactant 2

HCID 700EthanolamineHCID 15395954-Sulfanylidene-1,3-thiazolidin-2-one

Product 1

HCID 178518158HCID 178518158, compoundYield 70%

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

To a solution of 4-thioxothiazolidin-2-one (2.66 g) in ethanol (50 mL) was added 2-aminoethanol (1.22 g) at room temperature. The reaction mixture was stirred at room temperature for 4 hr, and the precipitate was collected by filtration and washed with ethanol to give the title compound (2.24 g).

Workup

  1. filtrationthe precipitate was collected by filtration
  2. washwashed with ethanol

Sources & evidence

ORD record
ord-a60c87c4a6b84791a22966203c880061
Source dataset
uspto-grants-2014_07
Patent number
US08772277B2

Reaction notes

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