HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1621059Generated: October 27, 2026
Ethylene Glycol → 2-Hydroxyethyl ethylpropenyl-phosphinate
https://huagongshe.com/reaction/1621059
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethylene Glycol | HCID 174 | — |
| Reactant | Butyl ethylpropenylphosphinate | HCID 86657322 | — |
| Catalyst | Dipotassium;bis(2-hydroxy-2-oxoacetate);oxotitanium;hydrate | HCID 91886499 | — |
| Product | 2-Hydroxyethyl ethylpropenyl-phosphinate | HCID 86657324 | 98% |
Reaction Steps
To 570 g (3.0 mol) of butyl ethylpropenylphosphinate (produced as in Example 6) are added 248 g (4 mol) of ethylene glycol and 0.4 g of potassium titanyl oxalate followed by stirring at 100° C. for 2 h. Volatiles are distilled off by gradual evacuation to leave 506 g (98% of theory) of 2-hydroxyethyl ethylpropenyl-phosphinate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08772519B2 |
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| Source dataset | uspto-grants-2014_07 |
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| ORD ID | ord-21d86f61c9c941bfa118012c2672cdaa |
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| Source note | uspto-grants-2014_07 |
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