HuagongsheHuagongshe Chemistry Print Report · For research reference only
Titanium tetrabutoxide → HCID 131731660, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Titanium tetrabutoxide | HCID 21801 | — |
| Reactant | HCID 57765530 | HCID 57765530 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 131731660 | HCID 131731660 | 92% |
Reaction Steps
134 g (1 mol) of ethylpropenylphosphinic acid (produced as in Example 12) and 85 g of titanium tetrabutoxide are refluxed in 500 ml of toluene for 40 hours. The resulting butanol is distilled off from time to time with proportions of toluene. The solution formed is subsequently freed of solvent to leave 133 g (92% of theory) of ethylpropenylphosphinic acid titanium salt.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08772519B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-e24687dfa2ae4a5b8ed52d7d60fc7dda |
| Source note | uspto-grants-2014_07 |