Sodium Azide → HCID 71279134, compound

HRID 1621137Notes

Reaction equation

HRID 1621137 reaction equation
CS(O[CH2:6][CH2:7][C:8]1[N:9]=[C:10]([C:14]2[CH:19]=[CH:18][N:17]=[C:16]([CH2:20][CH3:21])[CH:15]=2)[S:11][C:12]=1[CH3:13])(=O)=O.[N-:22]=[N+:23]=[N-:24].[Na+]>>[N:22]([CH2:6][CH2:7][C:8]1[N:9]=[C:10]([C:14]2[CH:19]=[CH:18][N:17]=[C:16]([CH2:20][CH3:21])[CH:15]=2)[S:11][C:12]=1[CH3:13])=[N+:23]=[N-:24]

Participants

3

Reactant 2

HCID 33557Sodium AzideHCID 86677488HCID 86677488, compound

Product 1

HCID 71279134HCID 71279134, compound

Procedure

The product was obtained starting from 2-(2-(2-ethylpyridin-4-yl)-5-methylthiazol-4-yl)ethyl methanesulfonate (226 mg, 692 μmol) and sodium azide (63.0 mg, 969 μmol) according to the method described in example 46, step 2 as light yellow oil (138 mg, 505 μmol, 72.9%).

Workup

  1. customThe product was obtained

Sources & evidence

ORD record
ord-14f7eefe431a4748ac9494457a34aae4
Source dataset
uspto-grants-2014_07
Patent number
US08772510B2

Reaction notes

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