HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Phenylprop-2-Enal → HCID 71451970, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Phenylprop-2-Enal | HCID 307 | — |
| Reactant | Benzeneacetamide | HCID 7680 | — |
| Reactant | HCID 71457306 | HCID 71457306 | — |
| Product | HCID 71451970 | HCID 71451970 | 88% |
Reaction Steps
Compound 46 was prepared from 2-phenylacetamide and cinnamaldehyde using the procedure for compound 44. Yield: 88%. 1H NMR (400 MHz, DMSO-d6) δ 8.61 (d, J=7.6 Hz, 2H), 7.21-7.37 (m, 15H), 6.41-6.45 (m, 1H), 6.27-6.32 (m, 1H), 6.04-6.09 (m, 1H), 3.44-3.52 (m, 4H). LCMS (ESI): m/z 385.1 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08772541B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-bae31a8383434a7a8c537cf0fdc61d63 |
| Source note | uspto-grants-2014_07 |