HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Aminophenol → HCID 66599953, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Aminophenol | HCID 11568 | — |
| Reactant | HCID 86647047 | HCID 86647047 | — |
| Product | HCID 66599953 | HCID 66599953 | — |
Reaction Steps
The title compound was prepared in an analogous manner to that described above in Example 22, Step 2 using 1-((5,6-dichloropyridin-3-yl)methyl)-4-(methylsulfonyl)piperazine and 3-aminophenol under microwave irradiation conditions (150° C., 30 min), and isolated as a pale yellow solid (70%). LCMS (API-ES) m/z 398 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08772480B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-57c10a4d6bdb4b02a690798c3b8c34e1 |
| Source note | uspto-grants-2014_07 |