NoName_3327 → N-(3-(4-Amino-6-methyl-1,3,5-triazin-2-YL)-5-methylpyridine-2-YL)-1H-indazol-4-amine

Participants

Role	Name	HCID	Charge
Reactant	NoName_3327	HCID 413085	—
Reactant	4-(2-Chloro-5-methylpyridin-3-yl)-6-methyl-1,3,5-triazin-2-amine	HCID 59548241	—
Product	N-(3-(4-Amino-6-methyl-1,3,5-triazin-2-YL)-5-methylpyridine-2-YL)-1H-indazol-4-amine	HCID 49786007	—

Reaction Steps

The experimental procedure for this compound was the same as Example 22, Step 2 using 4-(2-chloro-5-methylpyridin-3-yl)-6-methyl-1,3,5-triazin-2-amine and 1H-indazol-4-amine. LCMS (API-ES) m/z 333 (M+H)+. 1H NMR (400 MHz, d6-DMSO) δ 13.08 (d, J=2.35 Hz, 1H); 12.12 (br. s., 1H); 8.64 (br. s., 1H); 8.28 (dd, J=3.81, 2.05 Hz, 1H); 8.14 (d, J=5.28 Hz, 2H); 7.74 (br. s., 2H); 7.31 (d, J=7.63 Hz, 1H); 7.32 (br. s., 1H); 7.13 (d, J=12.91 Hz, 1H); 3.32 (d, J=1.37 Hz, 6H).

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US08772480B2
Source dataset	uspto-grants-2014_07
ORD ID	ord-fbe17c03ad3f440f8e15af67756c1ca2
Source note	uspto-grants-2014_07