HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 3-Methyl-1-[methyl(propan-2-yl)carbamoyl]-1H-imidazol-3-ium iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | N-isopropyl-N-methyl-1H-imidazole-1-carboxamide | HCID 66611115 | — |
| Product | 3-Methyl-1-[methyl(propan-2-yl)carbamoyl]-1H-imidazol-3-ium iodide | HCID 43145420 | — |
Reaction Steps
To a 50 mL round-bottomed flask was added N-isopropyl-N-methyl-1H-imidazole-1-carboxamide (0.550 g, 3.29 mmol), acetonitrile (29 mL, 3.29 mmol), iodomethane (0.817 mL, 13.16 mmol). The resulting solution was stirred at room temperature overnight. The solvent was removed under vacuum to afford 1-(isopropyl(methyl)carbamoyl)3-methyl-1H-imidazol-3-ium iodide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08772480B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-be8ae914ed0646e48b5e98073a57cea1 |
| Source note | uspto-grants-2014_07 |