HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → 3-bromo-2-hydroxy-5-methylbenzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | Benzaldehyde, 2-hydroxy-5-methyl- | HCID 69184 | — |
| Product | 3-bromo-2-hydroxy-5-methylbenzaldehyde | HCID 2757015 | 76.1% |
Reaction Steps
Proceeding as in Reference 9, but substituting 5-methyl salicylaldehyde (3 g, 22 mmol) and N-bromosuccinimide (4.7 g, 26.4 mmol), gave 3-bromo-2-hydroxy-5-methylbenzaldehyde (3.6 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08778625B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-d91f1f20221f4392a8c46ae24f4f4d27 |
| Source note | uspto-grants-2014_07 |