3-Nitrophenylboronic Acid → 5-Formyl-6-methoxy-3'-nitro-biphenyl-3-sulfonamide

HRID 1622124Notes

Reaction equation

HRID 1622124 reaction equation
Br[C:2]1[CH:3]=[C:4]([S:12]([NH2:15])(=[O:14])=[O:13])[CH:5]=[C:6]([CH:10]=[O:11])[C:7]=1[O:8][CH3:9].[N+:16]([C:19]1[CH:20]=[C:21](B(O)O)[CH:22]=[CH:23][CH:24]=1)([O-:18])=[O:17]>>[CH:10]([C:6]1[CH:5]=[C:4]([S:12]([NH2:15])(=[O:14])=[O:13])[CH:3]=[C:2]([C:23]2[CH:22]=[CH:21][CH:20]=[C:19]([N+:16]([O-:18])=[O:17])[CH:24]=2)[C:7]=1[O:8][CH3:9])=[O:11]

Participants

3

Reactant 2

HCID 16773-Nitrophenylboronic AcidHCID 866076983-Bromo-5-formyl-4-methoxy-benzenesulfonamide

Product 1

HCID 866077105-Formyl-6-methoxy-3'-nitro-biphenyl-3-sulfonamide

Procedure

Proceeding as in Reference 19, but substituting 3-bromo-5-formyl-4-methoxy-benzenesulfonamide and 3-nitrobenzene boronic acid, gave 5-formyl-6-methoxy-3′-nitro-biphenyl-3-sulfonamide.

Sources & evidence

ORD record
ord-588ef6066b794ba4ad2ea984c28437fd
Source dataset
uspto-grants-2014_07
Patent number
US08778625B2

Reaction notes

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