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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1622244Generated: October 31, 2026

Hydroxyamine hydrochloride → HCID 178421632, compound

https://huagongshe.com/reaction/1622244

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydroxyamine hydrochlorideHCID 443297—
ReactantHCID 86675684HCID 86675684—
ProductHCID 178421632HCID 178421632—

Reaction Steps

The title compound is prepared from (S)-4-[5-(1-methanesulfonyl-1,2,3,6-tetrahydro-pyridin-4-yl)-2-methyl-2,3-dihydro-furo[2,3-c]pyridin-2-yl]-piperidine-1-carbonitrile (Intermediate 42; the configuration of the stereocenter is arbitrarily assigned) and hydroxylamine hydrochloride following a procedure analogous to that described for Intermediate 11. LC (method 4): tR=0.46 min; Mass spectrum (ESI+): m/z=436 [M+H]+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08778926B2
Source datasetuspto-grants-2014_07
ORD IDord-f8a51fe330bd463d9ebc18b2adc63ec3
Source noteuspto-grants-2014_07