Hydroxyamine hydrochloride → HCID 178504932, compound

Participants

Reaction Steps

The title compound is prepared from (R)-4-[5-(1-methanesulfonyl-1,2,3,6-tetrahydro-pyridin-4-yl)-2,3-dihydro-furo[2,3-c]pyridine-2-yl]-piperidine-1-carbonitrile (Intermediate 44, the configuration of the stereocenter is arbitrarily assigned) and hydroxylamine hydrochloride following a procedure analogous to that described for Intermediate 11. LC (method 6): tR=0.75 min; Mass spectrum (ESI+): m/z=422 [M+H]+.

Provenance & Evidence