HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-5-ethylpyrazine → HCID 71208702, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-5-ethylpyrazine | HCID 45787628 | — |
| Reactant | HCID 67973217 | HCID 67973217 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 71208702 | HCID 71208702 | — |
Reaction Steps
The title compound is prepared from 5-(4-methanesulfonyl-phenyl)-2-piperidin-4-yl-2,3-dihydro-furo[2,3-c]pyridine and 2-bromo-5-ethylpyrazine in N,N-dimethylformamide following a procedure analogous to that described in Example 10. LC (method 5): tR=1.25 min; Mass spectrum (ESI+): m/z=465 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08778926B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-c0b5c62eaed34bee9b9d8e4d8cbc3b78 |
| Source note | uspto-grants-2014_07 |