Butyryl chloride → HCID 71208860, compound

Participants

Reaction Steps

The title compound is prepared from (S)—N-hydroxy-4-[5-(1-methanesulfonyl-1,2,3,6-tetrahydro-pyridin-4-yl)-2-methyl-2,3-dihydro-furo[2,3-c]pyridin-2-yl]-piperidine-1-carboxamidine (Intermediate 43; the configuration of the stereocenter is arbitrarily assigned) and butyryl chloride following a procedure analogous to that described in Example 8. LC (method 4): tR=1.00 min; Mass spectrum (ESI+): m/z=488 [M+H]+.

Provenance & Evidence