HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86675688, compound → HCID 71208494, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86675688 | HCID 86675688 | — |
| Reactant | HCID 178449908 | HCID 178449908 | — |
| Product | HCID 71208494 | HCID 71208494 | — |
Reaction Steps
The title compound is prepared from (S)-4-[5-(1-methanesulfonyl-1,2,3,6-tetrahydro-pyridin-4-yl)-2,3-dihydro-furo[2,3-c]pyridine-2-yl]-piperidine-1-carbonitrile (Intermediate 46; the configuration of the stereocenter is arbitrarily assigned) and N-hydroxy-isobutyramidine following a procedure analogous to that described in Example 2. LC (method 6): tR=1.40 min; Mass spectrum (ESI+): m/z=474 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08778926B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-eb639b64bbc74a2e802a193180edd3f6 |
| Source note | uspto-grants-2014_07 |