Methanol → HCID 58378278, compound

Participants

Reaction Steps

General procedure B was subsequently followed using benzyl-4-(1-(tert-butoxycarbonyl)piperidine-4-carbonyl)piperazine-1-carboxylate (330 mg), MeOH (10 mL) and a 4 M solution of hydrogen chloride in 1,4-dioxane (10 mL) to furnish the title compound 12 as a white solid (120 mg, 46%), umax (CHCl3)/cm−1 3016, 2949, 1699, 1639, 1431, 1250, 1227, 1125, 1019; m/z (ESI) C18H26N3O3 requires 332.1969, found [M+H]+ 332.1968.

Provenance & Evidence