Triethylamine → HCID 23566910, compound

Participants

Reaction Steps

General procedure C was followed using N-methylpiperazine (27 mg, 0.27 mmol), 3,4,5-trichloropyridine (50 mg, 0.27 mmol), triethylamine (0.76 μL, 0.54 mmol) and NMP (1.5 mL). The crude product was purified by flash column chromatography on silica gel (hexane/EtOAc, 1:1) to furnish the title compound as a colourless oil (44 mg, 65%), umax (CHCl3)/cm−1 2942, 2849, 2803, 1558, 1449, 1289, 1151; m/z (ESI) C10H14Cl2N3 requires 246.0559, found [M+H]+ 246.0560.

Provenance & Evidence