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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1622798Generated: October 31, 2026

HCID 66748164, compound → HCID 66823919, compound

https://huagongshe.com/reaction/1622798

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 66748164HCID 66748164—
CatalystAdams' catalystHCID 345198—
SolventMethanolHCID 887—
ProductHCID 66823919HCID 6682391937.5%

Reaction Steps

A mixture of 9-(4-propoxyphenyl)-3,4-dihydropyrido[2,1-c][1,2,4]thiadiazine 2,2-dioxide (300 mg) and platinum(IV) oxide (32.1 mg) in MeOH (10 mL) was stirred at room temperature under H2 for 20 hr. The reaction mixture was filtered by Celite and the filtrate was concentrated in vacuo. The residue was recrystallized from EtOAc-MeOH to give the title compound (114 mg) as a white solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08778934B2
Source datasetuspto-grants-2014_07
ORD IDord-91c00817e9ae495b89979754d27b3bf2
Source noteuspto-grants-2014_07