Diethyl Ether → HCID 66922905, compound

Participants

Reaction Steps

To a solution of Intermediate 16 (0.05 g, 0.095 mmol) in DCM (2 ml) was added TFA (1 ml). The reaction mixture was stirred at RT for 5 hours and then concentrated under reduced pressure to leave a yellow oil. Trituration with Et2O afforded the title compound as an off-white solid (42 mg, 94%).

Provenance & Evidence