Benzyloxyamine hydrochloride → HCID 58869096, compound

Participants

Reaction Steps

By the general method described in Part F of Example 30, 5-(4-amino-2-methyl-1H-imidazo[4,5-c]quinolin-1-yl)pentan-2-one was reacted with O-benzylhydroxylamine hydrochloride to provide 5-(4-amino-2-methyl-1H-imidazo[4,5-c]quinolin-1-yl)pentan-2-one O-benzyloxime) in about a 3 to 1 mixture of E and Z isomers as white crystals after recrystallization from a mixture of toluene and hexane, mp 146-148° C.

Provenance & Evidence