Cyclohexanone → (1-Methoxycyclohexyl)methyl 4-methylbenzenesulfonate

HRID 1623249Notes

Reaction equation

[C:1]1(=O)CCCCC1.[CH3:8][C:9]1[CH:14]=[CH:13][C:12]([S:15]([O:18][CH2:19][C:20]2([O:26][CH3:27])[CH2:25][CH2:24]O[CH2:22][CH2:21]2)(=[O:17])=[O:16])=[CH:11][CH:10]=1>>[CH3:8][C:9]1[CH:14]=[CH:13][C:12]([S:15]([O:18][CH2:19][C:20]2([O:26][CH3:27])[CH2:25][CH2:24][CH2:1][CH2:22][CH2:21]2)(=[O:17])=[O:16])=[CH:11][CH:10]=1

Participants

Reactant 2

HCID 7967Cyclohexanone

HCID 58127128(4-methoxytetrahydro-2H-pyran-4-yl)methyl 4-methylbenzenesulfonate2×

Product 1

HCID 58127190(1-Methoxycyclohexyl)methyl 4-methylbenzenesulfonate

Procedure

This compound was synthesized from cyclohexanone following the procedure described for (4-methoxytetrahydro-2H-pyran-4-yl)methyl 4-methylbenzenesulfonate (Intermediate O).

Sources & evidence

ORD record: ord-2547af37cbf4417595ba391437a4ac27
Source dataset: uspto-grants-2014_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08778951B2

Reaction notes

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