HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Difluoro-4-iodobenzene → HCID 51033657, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Difluoro-4-iodobenzene | HCID 2724444 | — |
| Reactant | 3-{[Phenyl-(3-phenyl propynoyl)-amino]-methyl}-benzoic acid methyl ester | HCID 67036155 | — |
| Product | HCID 51033657 | HCID 51033657 | — |
Reaction Steps
The title compound was prepared in analogy to Example 5 starting from 1,2-difluoro-4-iodo-benzene (commercially available) and 3-{[phenyl-(3-phenyl propynoyl)-amino]-methyl}-benzoic acid methyl ester. 1H NMR (300 Hz, CDCl3): δppm 3.90 (s, 3H), 4.96 (s, 2H), 6.58 (d, 1H), 6.70 (m, 2H), 7.07-7.32 (m, 4H), 7.34-7.43 (m, 6H), 7.50 (d, 1H), 7.94 (d, 1H), 8.02 (s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08778973B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-f9e0288cf13f44f8accecd6abcf65fe5 |
| Source note | uspto-grants-2014_07 |