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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1623446Generated: November 1, 2026

1-Chloro-3-iodobenzene → HCID 51033658, compound

https://huagongshe.com/reaction/1623446

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-Chloro-3-iodobenzeneHCID 12269—
Reactant3-{[Phenyl-(3-phenyl propynoyl)-amino]-methyl}-benzoic acid methyl esterHCID 67036155—
ProductHCID 51033658HCID 51033658—

Reaction Steps

The title compound was prepared in analogy to Example 5 starting from 1-chloro-3-iodo-benzene (commercially available) and 3-{[phenyl-(3-phenyl propynoyl)-amino]-methyl}-benzoic acid methyl ester. 1H NMR (CDCl3, 300 MHz) δppm 8.01 (s, 1H), 7.93 (d, 1H), 7.50 (d, 1H), 7.26-7.46 (m, 10H), 7.08 (t, 1H), 6.70 (t, 1H), 6.65 (d, 1H), 6.44 (d, 1H), 4.96 (s, 2H), 3.90 (s, 3H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08778973B2
Source datasetuspto-grants-2014_07
ORD IDord-28eaf59e9931406db8457d26c9369664
Source noteuspto-grants-2014_07