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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1623447Generated: October 31, 2026

1-Chloro-2-iodobenzene → HCID 51033659, compound

https://huagongshe.com/reaction/1623447

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-Chloro-2-iodobenzeneHCID 11993—
Reactant3-{[Phenyl-(3-phenyl propynoyl)-amino]-methyl}-benzoic acid methyl esterHCID 67036155—
ProductHCID 51033659HCID 51033659—

Reaction Steps

The title compound was prepared in analogy to Example 5 starting from 1-chloro-2-iodo-benzene (commercially available) and 3-{[phenyl-(3-phenyl propynoyl)-amino]-methyl}-benzoic acid methyl ester. 1H NMR (CDCl3, 300 MHz) δppm 8.01 (s, 1H), 7.92 (d, 1H), 7.50-7.52 (m, 4H), 7.37-7.42 (m, 7H), 7.07 (t, 1H), 6.62-6.69 (m, 1H), 6.05 (d, 1H), 4.96 (dd, 2H), 3.91 (s, 3H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08778973B2
Source datasetuspto-grants-2014_07
ORD IDord-7d731c7627544262a2bd969698ec1c3e
Source noteuspto-grants-2014_07