HRID1623458

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID2801416

2-Iodothioanisole

C7H7IS

结构：COC(=O)c1cccc(CN(C(=O)C#Cc2ccccc2)c2ccccc2)c1

HCID67036155

未命名化合物

PRODUCTS

生成物

$结构：COC(=O)c1cccc(CN2C(=O)/C(=C(\c3ccccc3)c3ccccc3SC)c3ccccc32)c1$

HCID51034987

未命名化合物

PROCEDURE

实验过程

The title compound was prepared in analogy to Example 5 starting from 1-iodo-2-methylsulfanyl-benzene (commercially available) and 3-{[phenyl-(3-phenyl propynoyl)-amino]-methyl}-benzoic acid methyl ester. 1H NMR (300 Hz, CDCl3): δppm 2.31 (s, 3H), 3.90 (s, 3H), 5.00 (dd, 2H), 6.03 (d, 1H), 6.60-6.64 (m, 2H), 7.04 (t, 1H), 7.26-7.30 (m, 2H), 7.33-7.56 (m, 9H), 7.95 (d, 1H), 8.01 (s, 1H).