HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Acetylphenylboronic acid → HCID 51034667, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Acetylphenylboronic acid | HCID 3702122 | — |
| Reactant | HCID 67036178 | HCID 67036178 | — |
| Product | HCID 51034667 | HCID 51034667 | — |
Reaction Steps
The title compound was prepared in analogy to Example 84 starting from 4-acetyl-phenylboronic acid (commercially available) and 3-{[(2-iodo phenyl)-(4-methyl-pent-2-ynoyl)-amino]-methyl}-benzoic acid methyl ester. 1H NMR (CDCl3, 300 MHz) δppm 8.03-8.11 (m, 4H), 7.94 (d, 1H), 7.71 (d, 1H), 7.52 (d, 1H), 7.40 (t, 1H), 7.29 (d, 2H), 7.00 (t, 1H), 6.61 (d, 1H), 6.54 (t, 1H), 5.61 (d, H), 5.02-5.07 (m, 3H), 3.90 (s, 3H), 2.70 (s, 3H), 1.19 (d, 3H), 1.17 (d, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08778973B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-05e434d263dd464b9507b5e384e3bbd4 |
| Source note | uspto-grants-2014_07 |