HRID1623904

反应详情

EQUATION

反应方程式

HRID 1623904 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

10% Pd/C (10 mg) was added to (S)-4-(1-azido-2-(tert-butyldimethylsilyloxy)ethyl)pyridine (58 mg, 0.208 mmol) in methanol. The reaction was degassed, and then charged with hydrogen. The reaction was stirred at room temperature overnight and filtered. The filtrate was concentrated to give the title compound (50 mg) without further purification.

WORKUP

后处理

  1. customThe reaction was degassed
  2. additioncharged with hydrogen
  3. filtrationfiltered
  4. concentrationThe filtrate was concentrated