Propylene Oxide → 34091-34-4
Reaction equation
[CH3:1][C:2]1[NH:3][CH:4]=[CH:5][N:6]=1.[CH2:7]1[O:10][CH:8]1[CH3:9]>CO>[OH:10][CH:8]([CH3:9])[CH2:7][N:3]1[CH:4]=[CH:5][N:6]=[C:2]1[CH3:1]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
2-Methylimidazole (1 mol) and methanol as a solvent were charged into a stirring-type autoclave, and propylene oxide (1 mol) was reacted therewith at a reaction temperature of 80° C. to 140° C. Thereafter, by purification through distillation, 1-(2-hydroxypropyl)-2-methylimidazole was obtained.
Workup
- customwas reacted
- customat a reaction temperature of 80° C. to 140° C
- customThereafter, by purification
- distillationthrough distillation
Sources & evidence
- ORD record
- ord-a81c5a798584430f9b9f47f88edcb448
- Source dataset
- uspto-grants-2014_07
- Patent number
- US08779018B2
Reaction notes
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