Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 1-Oxo-6,7,8,9-tetrahydro-5H-1lambda~5~-cyclohepta[b]pyridine | HCID 589689 | — |
| Product | HCID 10081676 | HCID 10081676 | — |
Reaction Steps
The N-oxide was dissolved in acetic anhydride (222 mL) and heated at 90° C. overnight. The mixture was cooled to room temperature and concentrated. Distillation (Kugelrohr, bp 110-140° C. @ 1 Torr) of the resultant oil provided 53.26 g of acetic acid 6,7,8,9-tetrahydro-5H-cyclohepta[b]pyridin-9-yl ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08778967B2 |
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| Source dataset | uspto-grants-2014_07 |
|---|
| ORD ID | ord-1a3767a1795d4bc9bcc5b9c284856a62 |
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| Source note | uspto-grants-2014_07 |
|---|
