Benzyl azide → HCID 66579249, compound

HRID 1624414Notes

Reaction equation

HRID 1624414 reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[O:12][N:11]=[C:10]([CH3:13])[C:9]=2[CH:14]([OH:17])[C:15]#[CH:16])=[CH:4][CH:3]=1.[N:18]([CH2:21][C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1)=[N+:19]=[N-:20]>>[CH2:21]([N:18]1[CH:16]=[C:15]([CH:14]([C:9]2[C:10]([CH3:13])=[N:11][O:12][C:8]=2[C:5]2[CH:4]=[CH:3][C:2]([Br:1])=[CH:7][CH:6]=2)[OH:17])[N:20]=[N:19]1)[C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1

Participants

3

Reactant 2

HCID 12152Benzyl azideHCID 866524111-[5-(4-Bromo-phenyl)-3-methyl-isoxazol-4-yl]-prop-2-yn-1-ol

Product 1

HCID 66579249HCID 66579249, compound

Procedure

Prepared according to the procedure described in Example 25, Step 2, using 1-[5-(4-Bromo-phenyl)-3-methyl-isoxazol-4-yl]-prop-2-yn-1-ol (Enantiomer B) and azidomethyl-benzene.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-1ba148a9fa88401a9a42d9d591eb9bed
Source dataset
uspto-grants-2014_07
Patent number
US08778983B2

Reaction notes

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