HuagongsheHuagongshe Chemistry Print Report · For research reference only
{2-[(Dimethylamino)methyl]phenyl}boronic acid → HCID 66577776, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | {2-[(Dimethylamino)methyl]phenyl}boronic acid | HCID 2734345 | — |
| Reactant | HCID 66577668 | HCID 66577668 | — |
| Catalyst | Bis(cyclopenta-1,4-dien-1-yl(diphenyl)phosphane);dichloropalladium;iron(2+) | HCID 178418228 | — |
| Product | HCID 66577776 | HCID 66577776 | — |
Reaction Steps
Prepared according to the procedure described in Example 1, Step 10, using 1-{4′-[4-(3-bromo-phenylamino)-3-methyl-isoxazol-5-yl]-biphenyl-4-yl}-cyclopropanecarboxylic acid ethyl ester and 2-(N,N-dimethylaminomethyl)-phenylboronic acid. (1,1′-Bis(diphenylphosphino)ferrocene)-dichloropalladium(II) was used in place of tetrakis(triphenylphosphine)palladium(0).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08778983B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-24d80b1e544f40918e0f5276d70dc9b2 |
| Source note | uspto-grants-2014_07 |