HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(4-Benzyloxyphenyl)-heptane-1,3-dione → 1-(4-Hydroxyphenyl)heptane-1,3-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(4-Benzyloxyphenyl)-heptane-1,3-dione | HCID 66733697 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 1-(4-Hydroxyphenyl)heptane-1,3-dione | HCID 45275210 | — |
Reaction Steps
1-(4-Benzyloxyphenyl)-heptane-1,3-dione (4 g; see step (a) above) was dissolved in toluene (20 ml) and Pd/C (3%; 80 mg) was added. The mixture was stirred at room temperature until hydrogen uptake ceased. After filtration of the catalyst, the solvent was evaporated leaving 2.84 g, 100%, 1-(4-hydroxyphenyl)-heptane-1,3-dione.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08779201B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-7a24a42675fb4ef1b16634daddaed652 |
| Source note | uspto-grants-2014_07 |