Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | HCID 178526242 | HCID 178526242 | — |
| Product | HCID 178506294 | HCID 178506294 | 27% |
Reaction Steps
Phosphorus oxychloride (76.4 g) was gradually added to compound (1b) (33.2 g), followed by stirring at 100° C. for 1 hr. The reaction solution was poured into ice water, and sodium hydroxide was added thereto to adjust the pH to 10. The precipitate was collected by filtration to obtain compound (1c) (9.76 g, 27%) as a light pink solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08779142B2 |
|---|
| Source dataset | uspto-grants-2014_07 |
|---|
| ORD ID | ord-4fe16cff0d1d4058ade15650a02cba36 |
|---|
| Source note | uspto-grants-2014_07 |
|---|
