HCID 10315293, compound → HCID 9977404, compound

HRID 1625276Notes

Reaction equation

HRID 1625276 reaction equation
ClCCO[CH2:5][CH2:6][O:7][CH2:8][CH2:9][O:10][CH2:11][CH2:12][O:13][CH2:14][CH2:15][O:16][CH2:17][CH2:18][N:19]1[C:27](=[O:28])[C:26]2[C:21](=[CH:22][CH:23]=[CH:24][CH:25]=2)[C:20]1=[O:29].[Cl:30]CCOCCOCCOCCN1C(=O)C2C(=CC=CC=2)C1=O>>[Cl:30][CH2:5][CH2:6][O:7][CH2:8][CH2:9][O:10][CH2:11][CH2:12][O:13][CH2:14][CH2:15][O:16][CH2:17][CH2:18][N:19]1[C:27](=[O:28])[C:26]2[C:21](=[CH:22][CH:23]=[CH:24][CH:25]=2)[C:20]1=[O:29]

Participants

3

Reactant 2

HCID 10315293HCID 10315293, compoundHCID 10410402HCID 10410402, compound

Product 1

HCID 9977404HCID 9977404, compoundYield 92%

Procedure

2-{2-[2-(2-{2-[2-(2-Chloroethoxy)-ethoxy}-ethoxyl-ethoxy)-ethoxy]-ethyl}-isoindole-1,3-dione. The title compound was prepared according to the synthesis of 2-(2-{[2-(2-Chloro-ethoxy)-ethoxy]-ethoxy}-ethyl)-isoindole-1,3-dione in 92% yield: 1H NMR (CDCl3) δ 7.84 (dd, 2 H), 7.71 (dd, 2H), 3.90 (t, 2H), 3.74 (q, 4 H), 3.67-3.58 (m, 18H). Mass spectrum, m/e Calcd for C20H29ClNO7+: 430.16 (100.0%). Found: 429.85.

Sources & evidence

ORD record
ord-15b5a392ed634cbbb0a3e2259c06c1e5
Source dataset
uspto-grants-2014_07
Patent number
US08779221B2

Reaction notes

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