HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Bromobenzenesulfonyl chloride → 4-Bromo-benzenesulfonic acid (S)-2-(methyl-prop-2-ynyl-amino)-3-phenyl-propyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Bromobenzenesulfonyl chloride | HCID 7396 | — |
| Reactant | (2S)-2-[methyl(prop-2-yn-1-yl)amino]-3-phenylpropan-1-ol | HCID 57789236 | — |
| Product | 4-Bromo-benzenesulfonic acid (S)-2-(methyl-prop-2-ynyl-amino)-3-phenyl-propyl ester | HCID 86632945 | 47% |
Reaction Steps
Compound 4c is synthesized by general procedure K from 4b p-bromo-benzene sulfonyl chloride in 47% yield (1.58 g, 1.41 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08784775B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-77bfbb9f0c274f1ba0209de67f00b9a2 |
| Source note | uspto-grants-2014_07 |