HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → 3-(Benzylthio)-6-(2,4-dimethylphenyl)pyridazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | 6-(2,4-Dimethylphenyl)pyridazine-3-thiol | HCID 12562100 | — |
| Product | 3-(Benzylthio)-6-(2,4-dimethylphenyl)pyridazine | HCID 41526799 | — |
Reaction Steps
Prepared in a similar manner to example 13 using benzyl bromide and 6-(2,4-dimethylphenyl)pyridazine-3(2H)-thione (Example 13a). Yield 53.5 mg (38%). 1H NMR (300 MHz, dMSO): δ 2.29 (s, 3H), 2.34 (s, 3H), 4.60 (s, 2H), 7.16-7.17 (m, 2H), 7.30-7.34 (m, 4H), 7.47-7.49 (d, 2H), 7.64-7.72 (m, 2H); MS (M+H, 307).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08784782B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-7c4c7cd6bcc947c594a0b3c031bffcb5 |
| Source note | uspto-grants-2014_07 |