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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1625571Generated: October 31, 2026

Benzyl Bromide → 3-(Benzylthio)-6-(2,4-dimethylphenyl)pyridazine

https://huagongshe.com/reaction/1625571

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzyl BromideHCID 7498—
Reactant6-(2,4-Dimethylphenyl)pyridazine-3-thiolHCID 12562100—
Product3-(Benzylthio)-6-(2,4-dimethylphenyl)pyridazineHCID 41526799—

Reaction Steps

Prepared in a similar manner to example 13 using benzyl bromide and 6-(2,4-dimethylphenyl)pyridazine-3(2H)-thione (Example 13a). Yield 53.5 mg (38%). 1H NMR (300 MHz, dMSO): δ 2.29 (s, 3H), 2.34 (s, 3H), 4.60 (s, 2H), 7.16-7.17 (m, 2H), 7.30-7.34 (m, 4H), 7.47-7.49 (d, 2H), 7.64-7.72 (m, 2H); MS (M+H, 307).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08784782B2
Source datasetuspto-grants-2014_07
ORD IDord-7c4c7cd6bcc947c594a0b3c031bffcb5
Source noteuspto-grants-2014_07