Sodium Hydroxide → HCID 67364228, compound
Reaction equation
[NH:1]1[CH2:5][CH2:4][CH:3]=[C:2]1[C:6]([O:8]C)=[O:7].[OH-].[Na+:11]>>[NH:1]1[CH2:5][CH2:4][CH:3]=[C:2]1[C:6]([O-:8])=[O:7].[Na+:11]Participants
3
Procedure
Methyl pyrroline-2-carboxylate (2.265 g) was dissolved in 1 N NaOH(aq) (17.8 mL) and stirred at room temperature for 1 hour. The reaction mixture was lyophilized to give crude sodium pyrroline-2-carboxylate (3647-164) as a white powder. ESI-MS calculated for C5H7NO2 [MH]+: 114.1; observed: 114.2.
Sources & evidence
- ORD record
- ord-e23b4bd59fec4cd19354bf59337e7993
- Source dataset
- uspto-grants-2014_07
- Patent number
- US08785151B2
Reaction notes
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