5-Bromo-2-chlorobenzaldehyde → HCID 66608057, compound

HRID 1625825Notes

Reaction equation

HRID 1625825 reaction equation
[CH2:1]([O:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[C:10]1[S:11][CH:12]=[CH:13][CH:14]=1)[CH3:2].[Br:15][C:16]1[CH:17]=[CH:18][C:19]([Cl:24])=[C:20]([CH:23]=1)[CH:21]=O>>[Br:15][C:16]1[CH:17]=[CH:18][C:19]([Cl:24])=[C:20]([CH2:21][C:12]2[S:11][C:10]([C:5]3[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=3[O:3][CH2:1][CH3:2])=[CH:14][CH:13]=2)[CH:23]=1

Participants

3

Reactant 2

HCID 106089255-Bromo-2-chlorobenzaldehydeHCID 20514143HCID 20514143, compound

Product 1

HCID 66608057HCID 66608057, compound

Procedure

The above 2-(2-ethoxyphenyl)thiophene and 5-bromo-2-chlorobenzaldehyde obtained in Reference Example 16-(1) were treated in a manner similar to Reference Example 9 to give 5-bromo-2-chloro-1-(5-(2-ethoxyphenyl)-2-thienylmethyl)benzene as colorless oil. APCI-Mass m/Z 407/409 (M+H).

Workup

  1. additionwere treated in a manner similar to Reference Example 9

Sources & evidence

ORD record
ord-9847874bebc94d9cb93dcfaef0b5c215
Source dataset
uspto-grants-2014_07
Patent number
US08785403B2

Reaction notes

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