HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Phenylthiophene-2-carbaldehyde → 3-Bromo-2-fluoro-6-methyl-1-(5-phenyl-2-thienylmethyl)benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Phenylthiophene-2-carbaldehyde | HCID 177053 | — |
| Reactant | 4-Bromo-3-fluorotoluene | HCID 573280 | — |
| Product | 3-Bromo-2-fluoro-6-methyl-1-(5-phenyl-2-thienylmethyl)benzene | HCID 66608527 | — |
Reaction Steps
4-Bromo-3-fluorotoluene and 5-phenyl-2-thiophenecarboxaldehyde were treated in a manner similar to Reference Example 116 to give the target compound as pale blue powders. APCI-Mass m/Z 361/363 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08785403B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-2775d5371d9248baa9737e44f63fc4dd |
| Source note | uspto-grants-2014_07 |