HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,5-Dibromopyridine → 5-Bromo-2-chlorophenyl 6-bromo-3-pyridyl ketone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,5-Dibromopyridine | HCID 69353 | — |
| Reactant | 5-Bromo-2-chloro-N-methoxy-N-methylbenzamide | HCID 53418379 | — |
| Product | 5-Bromo-2-chlorophenyl 6-bromo-3-pyridyl ketone | HCID 46930335 | — |
Reaction Steps
The above N-methoxy-N-methyl-5-bromo-2-chlorobenzamide and 2,5-dibromopyridine were treated in a manner similar to Reference Example 31-(4) to give 5-bromo-2-chlorophenyl 6-bromo-3-pyridyl ketone as a pale yellow solid. APCI-Mass m/Z 374/376 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08785403B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-e0a8c754527647848b8670fb10806f78 |
| Source note | uspto-grants-2014_07 |