3,4-Dichlorophenol → HCID 67324775, compound

Participants

Reaction Steps

103 mg of cesium carbonate and 100 mg of 5-methanesulfonyl-7-propoxy-2-(3-methyl-phenyl)-oxazolo[5,4-d]pyrimidine were added to a solution of 49 mg of 3,4-dichlorophenol in 3 ml of DMF. The mixture was stirred at room temperature for 2 h. After filtration, the solvent was distilled off in vacuo, and the product was isolated via preparative HPLC to yield 54 mg of the title compound.

Provenance & Evidence