HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexanol → HCID 67324303, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexanol | HCID 7966 | — |
| Reactant | Cesium carbonate | HCID 10796 | — |
| Reactant | HCID 67175734 | HCID 67175734 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 67324303 | HCID 67324303 | 9.5% |
Reaction Steps
113 mg of cesium carbonate and 100 mg of 5-methanesulfonyl-7-propoxy-2-(3-methyl-phenyl)-oxazolo[5,4-d]pyrimidine were added to a solution of 29 mg of cyclohexanol in 3 ml of DMF. The mixture was stirred at room temperature for 18 h. After filtration, the solvent was distilled off in vacuo, and the product was isolated via preparative HPLC to yield 10 mg of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08785439B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-0d4e1c07447a4e31b889afe0d279d3a0 |
| Source note | uspto-grants-2014_07 |