HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl bromodifluoroacetate → HCID 67234404, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl bromodifluoroacetate | HCID 69585 | — |
| Reactant | [N(E),S(R)]-N-[1-(5-Bromo-2-fluorophenyl)ethylidene]-2-methyl-2-propanesulfinamide | HCID 87126877 | — |
| Product | HCID 67234404 | HCID 67234404 | — |
Reaction Steps
Starting from (R)-2-methyl-propane-2-sulfinic acid [1-(2-fluoro-5-bromo-phenyl)-(E)-ethylidene]-amide (intermediate A2.1) and ethyl 2-bromo-2,2-difluoroacetate, the product (3R)-ethyl 3-((R)-1,1-dimethylethylsulfinamido)-2,2-difluoro-3-(2-fluoro-5-bromo-phenyl)butanoate was obtained as an orange oil. MS (ISP): m/z=446.1 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08785436B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-9f34c33a2f914b51bdef803ede945e09 |
| Source note | uspto-grants-2014_07 |