Methanol → HCID 178448939, compound

Participants

Reaction Steps

To a solution of 3-(4-Boc-piperazin-1-yl)-1,9-dimethylphenothiazin-5-ium triiodide (158 mg, 0.2 mmol) in methanol (5 mL) methyl(n-butyl)amine (0.065 mL, 25.2 mg, 0.6 mmol) was added. Reaction mixture was stirred for 24 h at room temperature. The resulting mixture was concentrated to dryness and purified by flash chromatography using the methanol-chloroform gradient to provide the title compound.

Provenance & Evidence