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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1626764Generated: October 31, 2026

HCID 66679850, compound → HCID 46935601, compound

https://huagongshe.com/reaction/1626764

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 66679850HCID 66679850—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 46935601HCID 4693560181%

Reaction Steps

55 mg (0.13 mmol) of 5-(cyclohexylethynyl)-2-{[(4-cyclohexylphenyl)carbonyl]amino}benzoic acid obtained in Example 92 and 55 mg of Pd—C were stirred in ethanol (4 mL) at room temperature for 5 days. Thereafter, the mixture was filtered, and the filtrate was condensed, thereby giving 45 mg of the target 5-(2-cyclohexylethyl)-2-{[(4-cyclohexylphenyl)carbonyl]amino}benzoic acid (yield: 81%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08785473B2
Source datasetuspto-grants-2014_07
ORD IDord-91ac06fe5f804946a968b56179b099a7
Source noteuspto-grants-2014_07