HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromo-2-iodotoluene → HCID 68193185, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromo-2-iodotoluene | HCID 2724601 | — |
| Reactant | HCID 68193209 | HCID 68193209 | — |
| Product | HCID 68193185 | HCID 68193185 | 34% |
Reaction Steps
In accordance with Example 19-(2), but using [(4-bromo-2-methylbenzyl)oxy](tert-butyl)dimethylsilane instead of tert-butyl 5-(benzyloxy)-2-{[1-(5-bromopyridin-2-yl)piperidin-4-yl]methyl}-6-methylpyrimidine-4-carboxylate, and 4-bromo-1-iodo-2-methylbenzene instead of tert-butyl[(4-iodobenzyl)oxy]dimethylsilane, the title compound (yield 34%) was afforded as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08785462B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-4cef857564fc4607a6a286b486fb3d5b |
| Source note | uspto-grants-2014_07 |