反应详情

温度

160 °C

A mixture of compounds D3 (2 g, 13.41 mmol) and D4 (6.69 g, 33.5 mmol) in EtOH (10 ml) was subjected to microwave heating at 160° C. for 45 min. The reaction mixture was cooled to room temperature and then diluted with DCM, causing a solid to precipitate. The solid obtained was filtered off, washed thoroughly with DCM and dried in vacuo to yield compound D5 (2.65 g, 84%) as a pale yellow solid.

1. temperatureThe reaction mixture was cooled to room temperature
2. customto precipitate
3. customThe solid obtained
4. filtrationwas filtered off
5. washwashed thoroughly with DCM
6. customdried in vacuo